您的位置: 专家智库 > >

国家自然科学基金(21275091)

作品数:2 被引量:1H指数:1
相关作者:闫李霞康琪更多>>
相关机构:山东师范大学更多>>
发文基金:国家自然科学基金国家教育部博士点基金更多>>
相关领域:理学自动化与计算机技术更多>>

文献类型

  • 2篇中文期刊文章

领域

  • 2篇理学
  • 1篇自动化与计算...

主题

  • 1篇液相
  • 1篇液相色谱
  • 1篇液相色谱法
  • 1篇液相色谱法测...
  • 1篇乳粉
  • 1篇色谱
  • 1篇色谱法
  • 1篇色谱法测定
  • 1篇配方乳粉
  • 1篇相色谱
  • 1篇邻苯二甲酸酯
  • 1篇高效液相
  • 1篇高效液相色谱
  • 1篇QUARTZ
  • 1篇SEPARA...
  • 1篇IMPEDA...
  • 1篇RESONA...
  • 1篇IODINE
  • 1篇IMIDAZ...

机构

  • 1篇山东师范大学

作者

  • 1篇康琪
  • 1篇闫李霞

传媒

  • 1篇山东师范大学...
  • 1篇Chines...

年份

  • 2篇2015
2 条 记 录,以下是 1-2
排序方式:
液相色谱法测定乳粉中13种邻苯二甲酸酯被引量:1
2015年
本文建立了可用于婴幼儿配方乳粉中13种邻苯二甲酸酯类环境激素测定的超高效液相色谱-二极管阵列紫外检测器分析方法.样品经甲醇饱和正己烷超声提取、柱分离富集与净化后,以乙腈和水为流动相进行梯度洗脱.所检测的13种邻苯二甲酸酯的线性范围为0.5-50 mg/L,检测下限在0.05-0.4 mg/L之间,加标回收率为92-102%,相对标准偏差均小于10%,该方法操作简便、分析时间短、灵敏度高,适用于婴幼儿配方乳粉中邻苯二甲酸酯的筛查分析.
康琪闫李霞张贞理
关键词:邻苯二甲酸酯高效液相色谱配方乳粉
Monitoring iodine adsorption onto zeolitic-imidazolate framework-8 film using a separated-electrode piezoelectric sensor
2015年
In this work, a separated-electrode piezoelectric sensor(SEPS), constructed by a naked quartz crystal mounted between two electrodes, is reported for applications in a corrosive gaseous phase. The response of SEPS was measured by an impedance analysis method. It was shown that SEPS has an excellent frequency stability because its quality factor is in the order of 10^5. The SEPS can be operated even with the electrode gap in air larger than 1 cm. Compared with a conventional quartz crystal microbalance, the resonant frequency of the SEPS is independent of the mass change in the electrode. The SEPS was applied to monitor the adsorption of iodine on quartz surface and zeolitic-imidazolate framework-8(ZIF-8) film as well as in the transfer of iodine between two ZIF-8 films. The SEPS offers the advantages of easy preparation, corrosion-resistant and convenience in combination with mass and optical measurements.
Da-Zhong ShenTing-Ting CaiXi-Lei ZhuXiao-Long MaLing-Qiang KongQi Kang
共1页<1>
聚类工具0